A modified method is presented1 for the efficient extraction of pesticides from human adipose tissue. The procedure combines purification, extraction on Extrelut column and GC/MS analysis. This extraction procedure for pesticides in human adipose tissue was evaluated on the basis of accuracy, reproducibility, and chromatographic profile. The method is simple and rapid and produces relatively clean extracts, suitable for gas chromatography/mass spectrometry full scan EI analysis. The acidic purification/solid-phase extraction provided best compromise between recovery and chromatographic profile.
Simultaneous extraction of pesticides from human adipose tissues and GC/MS detection
GAGLIANO CANDELA R;AVENTAGGIATO, Lucia;STRISCIULLO G;COLUCCI A. P.
2007-01-01
Abstract
A modified method is presented1 for the efficient extraction of pesticides from human adipose tissue. The procedure combines purification, extraction on Extrelut column and GC/MS analysis. This extraction procedure for pesticides in human adipose tissue was evaluated on the basis of accuracy, reproducibility, and chromatographic profile. The method is simple and rapid and produces relatively clean extracts, suitable for gas chromatography/mass spectrometry full scan EI analysis. The acidic purification/solid-phase extraction provided best compromise between recovery and chromatographic profile.File in questo prodotto:
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